Specification:
SPIN INNING BASKET REACTOR APPARATUS
Description
Any catalytic liquid-liquid orliquid-gas reaction involving the use of a catalyst placed in basket can bestudies in this set-up.
Kinetic parameter of a specificreaction can be estimated & parametric studies can be conducted.
The set-up consists of a reactorcentrally having one spinning basket derived through a variable speed motor.The metered flow of reactant from feed tank is fed to the reactor at thebottom.
The set-up can be used as batch wiseof as continuous type. Sampling points are provided for analysis. Portconnection for gas inlet is provided at the bottom of the reactor
Experimentation/Learning Objectives
To determine the kinetic parametersfor a given reaction
Utilities Required
Electricity Supply: Single Phase, 220 V AC, 50 Hz, 5-15Amp combined socket with earth connection. Earth voltage should be less than 5volts.
Compressed air supply@1 Bar.
Water Supply.
Floor Drain.
Floor Area Required: 1.0 m x 0.75 m.
Instruments, Laboratory Glassware andChemicals required for analysis as per the system adopted
Technical Details
Reactor Vessel: Material Stainless Steel Effective Volume: 1000ml.
Basket: Material Stainless Steel, Fitted with appropriate StainlessSteel.
Drive for Basket: DC Motor with Thyristor controlledDC Drive for Variable Speed.
Packing: Catalyst
Feed Tank (1Nos.): Material Stainless Steel, Capacity10 Ltrs.
Flow Measurement: By Rotameter
Pressure regulator: Range 0-2 kg/cm
Pressure Gauge: Bourdon Type, 0-2 kg/cm
Receiver: Material Stainless Steel, Capacity 10 Ltrs.
Piping: Stainless Steel and PVC.
Hot water Circulation: Magnetic Pump of Poly propylene (inouter Jacket) to circulate Hot Water maximum working temp. 85C
Hot water tank: Made of Stainless Steel, Double wall, insulatedwith Ceramic Wool.
Capacity: 10-15 ltrs.






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