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ISOTHERMAL SEMI-BATCH REACTOR APPARATUS

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MOQ : 1 Piece

ISOTHERMAL SEMI-BATCH REACTOR APPARATUS Specification

Measuring Range
0-100% conversion, 0-2L volume

Interface Type
Analog/Digital

Power Supply
230 V AC, 50 Hz

Display Type
Digital LED

Hardness
n/a (not applicable)

Test Range
Up to 2 L batch volume

Accuracy
1% F.S.

Humidity
Up to 90% RH (non-condensing)

Application
Engineering Testing Equipment

Number of Specimens
1 (single reactor)

Usage
Engineering Testing Equipment

Product Type
ISOTHERMAL SEMI-BATCH REACTOR APPARATUS

Frequency
50 Hz

Temperature
Ambient to 80C (controlled)

Automation Grade
Semi-Automatic

Equipment Type
ISOTHERMAL SEMI-BATCH REACTOR APPARATUS

Operating Voltage
230 V AC

Max Height
600 mm

Specimen Size
Variable, up to 2 L

Port Size
12 mm (reactor input/output)

Response Time
<1 second

Mounting Type
Table-top

Features
Double-walled reactor, precise temperature control, variable feed input, stirring mechanism, over-temperature protection

Resolution
0.1 ml (feed measurement)

Gas Pressure
0-2 bar

Capacity
2 Liters (reactor volume)

Machine Weight
Approximately 40 kg

Test Speed
Adjustable, up to 100 rpm (agitator speed)

Test Width
150 mm

Test Stroke
100 mm

Control Mode
Manual/Automatic

Agitator Type
Magnetic/Mechanical Stirrer

Temperature Sensor
PT-100 RTD

Safety Features
Over-temperature cutoff, emergency stop

Thermal Insulation
Provided

Dimensions (LWH)
450 300 600 mm

Pressure Gauge
0-2 bar bourdon type

Sampling Port
Provided

Reactor Material
Borosilicate Glass / Stainless Steel

Reactor Vessel Lid
Flanged, with multiple ports

Feed System
Graduated feed tank with controlled dropping funnel

Instruction Manual
Included

ISOTHERMAL SEMI-BATCH REACTOR APPARATUS Trade Information

Minimum Order Quantity
1 Piece

Payment Terms
Cash on Delivery (COD), Cash Advance (CA), Cheque, Telegraphic Transfer (T/T), Letter of Credit (L/C)

Packaging Details
Carton Box, Export Quality also Available

Main Export Market(s)
Asia, Middle East, Africa

Main Domestic Market
All India

Certifications
ISO 9001, 14001, CE

About ISOTHERMAL SEMI-BATCH REACTOR APPARATUS

Specification:

ISOTHERMAL BATCH REACTOR APPARATUS

Description:

An isothermal semi-batch reactor is asemi-closed system with one input stream. It is operated under conditions likeIsothermal (Temperature of Reaction Mass remains constant) and perfectly mixed(composition of reaction mixture is uniform throughout).

This set-up is used to study anon-catalytic homogeneous reaction under isothermal condition. The set up consistsof a Reactor fitted in a constant temperature water bath. Before starting the reaction,the reactor is charged with measured quantity of one reactant.

From a feed tank another reactant isfed to the reactor. Using a sampling pipette samples can be taken out foranalysis after fixed interval. Peristaltic Pumps are provided to measure theindividual flow of Chemicals. One stirrer is fitted for mixing the reactants inreactor and other is fitted in water bath to keep the uniform temperaturethroughout in the bath. The temperature of bath can be maintained from ambientto 70C with the help of Digital Temperature indicator Cum Controller.

Experimentation:

To study a second ordersaponification reaction in a Semi-Batch Reactor.

To determine the Reaction RateConstant.

Product Details:

Voltage: 220 Volt (v)

Power: 500 Watt (w)

Material: Metal

Usage: For Laboratory

Equipment Materials: SS

Precise Temperature and Process Control

This reactor apparatus provides exceptional temperature regulation from ambient up to 80C, utilizing double-walled insulation and a PT-100 RTD sensor. The system enables controlled feed introduction through a graduated tank and dropping funnel, paired with adjustable magnetic or mechanical stirring, ensuring uniform mixing and accurate reaction data. The digital interface and selectable manual or automatic control offer flexibility in operation.

Safety Features and Robust Construction

Safety is a priority, with an over-temperature cutoff, emergency stop button, and double-walled reactor design. Its borosilicate glass or stainless steel construction ensures chemical resistance and durability. The flanged vessel lid includes multiple ports for sampling, pressure measurement, and reagent addition, while the bourdon-type pressure gauge provides real-time monitoring. This apparatus is built for consistent performance under demanding laboratory conditions.

Versatile Applications and User Benefits

Ideal for engineering education, research, and industrial process development, this semi-batch reactor accommodates single specimens up to 2 liters. Users benefit from a comprehensive instruction manual, variable feed input, high-resolution (0.1 ml) measurement, and rapid response time (<1 second). This facilitates in-depth kinetic studies, optimization, and scale-up of chemical processes, making it a valuable resource for laboratories and manufacturers.

FAQs of ISOTHERMAL SEMI-BATCH REACTOR APPARATUS:

Q: How do I operate the Isothermal Semi-Batch Reactor for a typical experiment?

A: Begin by assembling the reactor using the included instruction manual, ensuring all ports are securely fitted. Add the required reactants to the vessel, adjust the feed system to deliver input batches through the controlled dropping funnel, set the desired agitation speed (up to 100 rpm), and program temperature controls. Monitor progress via the digital LED display and utilize the sampling port to collect reaction samples at intervals.

Q: What materials is the reactor vessel made from and what are its advantages?

A: The reactor vessel is constructed from high-quality borosilicate glass or stainless steel. Borosilicate glass provides excellent chemical resistance and thermal stability, while stainless steel enhances durability and allows operation with a broader range of reagents and process conditions, ensuring reliability in chemical testing and industrial applications.

Q: When should the safety features be utilized during operation?

A: Safety features such as the over-temperature cutoff and emergency stop should be engaged anytime abnormal conditions arise, such as rapid temperature increases or equipment malfunction. Routine use of these features ensures operator safety and protects the apparatus from damage during unforeseen incidents.

Q: Where is the apparatus best installed for optimal performance?

A: This semi-batch reactor is designed as a table-top unit and should be placed on a stable, level surface in a well-ventilated laboratory or research facility. Ensure proximity to a 230 V AC, 50 Hz power supply, and that humidity does not exceed 90% RH (non-condensing) to maintain performance and user safety.

Q: What benefits does the variable feed system offer in engineering experiments?

A: The precisely controlled feed system allows users to add reactants at variable rates, enabling better control over reaction kinetics and process optimization. This flexibility enhances the study of semi-batch operations, supports detailed kinetic modeling, and aids in the scale-up of chemical processes from laboratory to industrial scale.

Q: How is process monitoring and data recording handled during reactor operation?

A: Process variables such as temperature, pressure (02 bar), and conversion rates are monitored in real-time via digital LED displays and accurate sensors. Measurements can be accessed via analog or digital interfaces, facilitating easy data recording for analysis, reporting, and process optimization.

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